Sintesis Senyawa Komponen Parfum Etil p-Anisat dari Anetol
| Main Authors: | KUSUMANINGSIH, TRIANA, Handayani, Desi Suci, MAKRUF, ANDI |
|---|---|
| Format: | Article PeerReviewed application/pdf |
| Terbitan: |
, 2004
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| Subjects: | |
| Online Access: |
http://eprints.uns.ac.id/857/1/197212071999032001biofarmasi3.pdf http://eprints.uns.ac.id/857/ |
Daftar Isi:
- Synthesis of ethyl p-anisate from anethole have been done. Ethyl p-anisate is ester coumpound which can use as perfume component. p-anisic acid was synthesized from anethole (1 mole) which oxidixed by KMnO4 (3 moles) at 40o C for 2 hours. Esterification with ethanol carried out at 78,5o C for 6 hours. Identification and determination structure coumpound of product synthesis used spectroscophic methodes (GC, GC-MS and IR). Anethole has been isolated from anise oil as 90,3%. p-Anisic acid and ethyl p-anisate as synthesized products got 45% and 79,9% respectively. Keywords: anethole, p-anisic acid, esterification, ethyl p-anisate.