EFFECT OF CONCENTRATION OF IMPERATA CYLINDRICA L LEAF EXTRACT ON SYNTHESIS PROCESS OF GOLD NANOPARTICLES
| Main Authors: | Syahjoko Saputra, Iwan, Yulizar, Yoki, Sudirman, Sudirman |
|---|---|
| Format: | Article info application/pdf eJournal |
| Bahasa: | ind |
| Terbitan: |
Center for Science & Technology of Advanced Materials - National Nuclear Energy Agency
, 2018
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| Subjects: | |
| Online Access: |
http://jurnal.batan.go.id/index.php/jsmi/article/view/4135 http://jurnal.batan.go.id/index.php/jsmi/article/view/4135/3637 http://jurnal.batan.go.id/index.php/jsmi/article/downloadSuppFile/4135/194 http://jurnal.batan.go.id/index.php/jsmi/article/downloadSuppFile/4135/195 http://jurnal.batan.go.id/index.php/jsmi/article/downloadSuppFile/4135/196 |
Daftar Isi:
- Gold Nanoparticles (GoldNPs) successful was performed using HAuCl4 precursor as Au3+ ion source with 7x10-4 M concentration. The research aims to knows effect of concentration variation of Imperata cylindrica L leaf extract on synthesis process of gold nanoparticles. The research used of green synthesis method. Colloid of nanoparticles which is formed in analyzed using UV-Vis Spectrophotometer, FT-IR Spectroscopy, PSA, PZC, XRD and TEM. The results of synthesis showed the best concentration of Imperata cilindrica L leaf extract at 3,46%, happen a shift of wavelength at UV-Vis from 216 nm to 530 nm with 1.779 absorbance value. The PSA analysis showed a particle size of 51.87 nm and a PZC value of -19.2 mV. The result of FT-IR indicated a shift of wavenumber in the hidroxyl group from 3354 cm-1 to 3390 cm-1 and showed a interaction of hydroxyl group at imperata cylindrica L leaf extract with Au3+ ion. TEM analysis shows the morphology of GoldNPs that spherical shape with a particle size of 20 nm. XRD calculation results show crystallite size of gold nanoparticles is 15.47 nm.