ANALISIS KESESUAIAN UJI KAPPA DENGAN MEMBANDINGKAN DUA METODE ANALISIS DELTAMETHRIN MENGGUNAKAN ALAT KROMATOGRAFI CAIR KINERJA TINGGI

Main Authors: , NISA HAKIMAH, , drh. R. Gagak Donny Satria, M.P., M.Pd.
Format: Thesis NonPeerReviewed
Terbitan: [Yogyakarta] : Universitas Gadjah Mada , 2014
Subjects:
ETD
Online Access: https://repository.ugm.ac.id/130195/
http://etd.ugm.ac.id/index.php?mod=penelitian_detail&sub=PenelitianDetail&act=view&typ=html&buku_id=70610
Daftar Isi:
  • Development of analysis using chromatography was shown by the appearance of High Performance Liquid Chromatography (HPLC) which can classified the organic chemical compound that didnâ��t vaporize with speed and high efficiency. Several of delthamethrin analysis method has been conducted in Pharmacology Department of Veterinary Medicine Faculty of Gadjah Mada University. This research intent on comparing and choosing delthamethrin analysis method using HPLC which has been developed by Pharmacology Laboratory of Veterinary Medicine Faculty of Gadjah Mada University and performing agreement analysis to the selected method by using kappa test. The instrument used as the analyzer in this research was a set of HPLC created by Shimadzu 6.1, SCL-10A VP system controled, the moving phase acetonitril Merck 80% in a sterile aquabidest, LC-10AD vP pump, collumn C18 Shim-Pack VP-ODS (150 x 4,6 mm) with temperature 300 C, injector, CTO-10C vP oven, UV-Vis SPD-10AV detector, DGU-14A degasser, and LC-10AV vP liquid chromatography. The material that used to the agreement analysis for the selected method is forty sampels of liver solution extract. The comparison result between method I and method II shows that method II gives a better result in analyzing deltamethrin. The agreement analysis result with kappa test shows a good agreement result (agreement value = 0,7).