KATALIS Pt/ZEOLIT DAN UJI AKTIVITASNYA TERHADAP REAKSI ESTERIFIKASI MINYAK JARAK (Ricinus communis)
Main Authors: | , ANKI NOVAIRI DARI, , Prof. Dr. Triyono, S.U. |
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Format: | Thesis NonPeerReviewed |
Terbitan: |
[Yogyakarta] : Universitas Gadjah Mada
, 2014
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Subjects: | |
Online Access: |
https://repository.ugm.ac.id/129616/ http://etd.ugm.ac.id/index.php?mod=penelitian_detail&sub=PenelitianDetail&act=view&typ=html&buku_id=70009 |
Daftar Isi:
- Esterification reaction of Castor oil (Ricinus communis) with ethanol and Pt/zeolite catalyst have been investigated. The objective of this study was to learn the effect and activity of Pt/zeolit catalyst for esterification reaction of castor oil. The first step pf the reaction was activation of Pt/zeolite catalyst by calcination then followed by esterification reaction. Esterification reaction was done by reacting castor oil and ethanol with Pt/zeolite catalyst in temperature 76°C for 6 hours. This reaction has been done by reflux process with castor oil : ethanol mol ratio = 1:12. Esters obtained from this reaction consists of glycerol and any other particulate matters which need to be separated by liquid-liquid extractions using warm aquadest (T=50°C). The second process was transesterification reaction using NaOH catalyst by reflux process in temperature 76°C for 2 hours. The usage of any different kinds of catalyst for this reaction Pt/zeolite, H-zeolite, H2SO4 and NaOH showed most yield 95,457 % obtained from NaOH catalyst and the fewest 82,706 % obtained from H-zeolites catalyst. Variation of Pt/zeolite catalyst used in this reaction from 1,5