NANOSPHERE SYNTHESIS BASED ON FERROFLUID AND POLY LACTIC ACID USING SONICATION METHOD
| Main Authors: | Hapsari, B. W.; Departemen Fisika, FMIPA-IPB Kampus IPB, Darmaga Bogor, ., Mujamilah; Pusat Teknologi Bahan Industri Nuklir (PTBIN)-BATAN Kawasan Puspiptek, Serpong, Tangerang 15314, Kurniati, M.; Departemen Fisika, FMIPA-IPB Kampus IPB, Darmaga Bogor, Sulungbudi, Grace Tj.; Pusat Teknologi Bahan Industri Nuklir (PTBIN)-BATAN Kawasan Puspiptek, Serpong, Tangerang 15314 |
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| Other Authors: | IPB - Institut Pertanian Bogor |
| Format: | Article application/pdf eJournal |
| Bahasa: | ind |
| Terbitan: |
BATAN
, 2013
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| Online Access: |
http://jurnal.batan.go.id/index.php/jsmi/article/view/1054 |
Daftar Isi:
- Synthesis study ofmagnetic nanospheres involving wetting, emulsification using sonication and evaporation process have been done. Sonications time were varied for 3 minutes, 4 minutes, 5 minutes, 6 minutes and 7 minutes. Phase analysis result by X-Ray Diffractometer (XRD) showed that Poly Lactic Acid (PLA) tend to change to amorphous phase which become more significant with sonication time. There was no ferrofluid phase change. Size distribution analysis using Scanning Electron Microscope (SEM) showed for longer sonication time, size of nanospherewere decreasing and becomemore homogeneous. Hysteresis curve from measurement using Vibration Sample Magnetometer (VSM) showed increasing of magnetization value with decreasing of nanosphere size, which analized due to higher loading factor of ferrofluid within nanosphere. From these three characterization results, it can be concluded that sample with sonication time of 4 minutes give an optimum nanosphere with respect to its size, homogeneity and the magnetic properties.Keywords: Magnetic nanosphere, Ferrofluid, Poly Lactic Acid, Sonication.