Separation and purification of cardol, cardanol and anacardic acid from cashew (Anacardium occidentale L.) nut-shell liquid using a simple two-step column chromatography

Main Authors: Yuliana, Maria, Thi, Bich Thuyen Nguyen, Faika, Sitti, Huynh, Lien Huong, Soetaredjo, Felycia Edi, Ju, Yi-Hsu
Format: Article PeerReviewed Book
Bahasa: eng
Terbitan: Taiwan Institute of Chemical Engineers , 2014
Subjects:
Online Access: http://repository.wima.ac.id/18205/1/2-Separation_and_purification_.pdf
http://repository.wima.ac.id/18205/7/2_Separation_and_hasil_cek_plagiasi_.pdf
http://repository.wima.ac.id/18205/13/2-R1%262_Separation_and_.pdf
http://repository.wima.ac.id/18205/
https://www.elsevier.com/locate/jtice
https://www.sciencedirect.com/science/article/pii/S1876107014002119?via%3Dihub
Daftar Isi:
  • Long chain phenols contained in cashew nut shell liquid have important applications. Anacardic acids and cardols are extensively used in the pharmaceutical industry, while cardanols find use in resins, coating and polymer industries. In this work, a two-step reversed-phase silica gel column chromatography was employed to purify these major phenols in cashew nut shell liquid (CNSL). 6- Pentadecyl salicylic acid (C22H36O3, 98.8% purity and 82.4% recovery), 5-pentadecyl resorcinol (C21H36O2, 99.3% purity and 80.7% recovery) and 3-pentadecyl phenol (C21H36O, 99.2% purity and 81.8% recovery) were successfully obtained and identified by 1H and 13C NMR, FTIR, mass spectrometry and elemental analysis.