An Investigation on Desilylation of Alkyl and Phenolic Silyl Ethers Using FeCI3
| Main Authors: | PARTHASARATHY SARAVANAN, VINOD K. SINGH |
|---|---|
| Format: | Article Journal |
| Bahasa: | eng |
| Terbitan: |
, 1998
|
| Subjects: | |
| Online Access: |
https://zenodo.org/record/5915449 |
Daftar Isi:
- Department of Chemistry, Indian Institute of Technology, Kanpur-208 016 Manuscript received 2 July 1998 A variety of alkyl and phenolic TBDMS ethers have been efficiently cleaved using anhydrous FeCI3 in MeOH under mild conditions. It was found that choice of solvent is crucial for the rate of the deprotection of TBDMS ether with FeCI3.