Synthesis of novel extractant and its application in extraction and separation studies of palladium(II) in hydrochloric acid medium
| Main Authors: | U. P. Shaikh, S. S. Katkar, K. N. Vidhate, M. K. Lande, B. R. Arbad |
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| Format: | Article Journal |
| Bahasa: | eng |
| Terbitan: |
, 2011
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| Subjects: | |
| Online Access: |
https://zenodo.org/record/5790410 |
Daftar Isi:
- 0epartment of Chemistry, Dr. Babasaheb Ambedkar Marathwada University, Aurangabad-431 004, Maharashtra, India E-mail : abr_chem@yahoo.co.in Millind College of Science, Nagsenvan, Aurangabad, Maharashtra, India Manuscript received 24 May 2010, revised 29 December 2010. accepted 12 January 2011 A simple and rapid liquid-liquid extraction of palladium(ll) studied involving complexation of palladium(ll) with 4-(4-ethoxybenzylideneamino)-5-methyi-4H-1,2,4-triazole-3-thiol (EBIMTT). The extraction was fast with short shaking time (30 s). The results obtained showed that the average recovery of palladium(ll) from an aquNms solution containing μg/ml of analyte was 99% with a relative standard deviation of 0.95. The method is applicable to the analysis of synthetic mixtures. It is highly selective, simple and rapid.