Synthesis and characterization of CrIII, FeIII, CoII, NiII, Cull and ZnII complexes of 2, 14-dimethyl-3, 15-di-n-propyl-1 ,4,13, 16- tetraazacyclotetracosa-1 ,3, 13,15-tetraene
| Main Authors: | R. N. Prasad, Mala Mathur |
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| Format: | Article |
| Bahasa: | eng |
| Terbitan: |
, 2011
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| Subjects: | |
| Online Access: |
https://zenodo.org/record/5766030 |
Daftar Isi:
- Department of Chemistry, University of Rajasthan, Jaipur-302 004, Rajasthan, India E-mail : rnp_1949@yahoo.co.in Manuscript received 31 December 2008, revised 08 July 2010, accepted 20 July 2010 CrIII, FeIII, Con, NiII, CuII and ZnII complexes of a 24-membered tetraazamacrocycle, 2,14-dimethyl-3,15- di-n-propyl-1,4,13,16-tetraazacyclotetracosa-1,3,13,15-tetraene, have been prepared by 2+2 cyclocondensation of 2,3- hexanedione and 1,8-diaminooctane in the presence of metal ions as templates. The complexes have been characterized by elemental anal}ses, conductances, IR spectra, magnetic measurements and 1H NMR spectra.