Sorption characteristics of mesoporous composite SiO2·TiO2

Main Authors: J.R. Uzokov, N.K. Mukhamadiev
Format: Article info application/pdf
Bahasa: eng
Terbitan: Central Asian Studies , 2021
Subjects:
Online Access: https://cajmns.centralasianstudies.org/index.php/CAJMNS/article/view/220
https://cajmns.centralasianstudies.org/index.php/CAJMNS/article/view/220/474
Daftar Isi:
  • Samples of mesoporous sorbents based on tetraethoxysilane and titanium dioxide in an acidic medium were  obtained using the sol-gel technology. The synthesized mesoporous sorbents are characterized by a large  specific surface area of 700-950 m2/g, as well as an average diameter of 2,6-6,5 nm and a low pore volume of 0,60-0,90 cm3/g. It was  found that a hysteresis loop is observed in the mesoporous sorbents during the adsorption of benzene and water vapors. The phase composition of the sorbents was   studied by X-ray diffractometry (XRD), surface characteristics by a scanning electron microscope (SEM). The mesoporous sorbents can be  used as a sorbent for gas chromatographic separation of light alkanes, olefins, aromatic hydrocarbons, alcohols, aldehydes, ketones, ethers and esters.