Sintesis dan karakterisasi sabun zink dari minyak sawit (Elaesis guinensis) dengan zink klorida / Muhammad Suba'i
| Main Author: | Suba'i, Muhammad |
|---|---|
| Format: | Thesis NonPeerReviewed |
| Terbitan: |
, 2010
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| Subjects: | |
| Online Access: |
http://repository.um.ac.id/24316/ |
Daftar Isi:
- ABSTRACTSubaiMuhammad.2009.SynthesisandCharacterizationofZincSoapfromPalmOil(Elaeisguinensis)withZincChloride.SkripsiChemistryFMIPAStateUniversityOfMalang.Instructor(1)Dr.SutrisnoM.Si(II)Dra.DedekSukarianingsihM.PdM.Si.Keywordzincsoappalmoiltrans-saponificationFirstconceptaboutsoapascarboxylicsaltfromionofalkalimetalhasbranchedoutbecomeothersoapwhichnotfromalkalimetalandhascharacteristicassoonasdifferentfunctionfromalkalimetalsoap.Aluminumsoapwassuccesssyntheticfromfatacidandnabatioilaspalmoilcastoroil.Oleatzincsoapandstearatzincsuccesssyntheticmakeuseofzincchloridewitholeatacidandstearatacid.Soneedfulresearchaboututilizationpalmoilassubstancesubstitutefatacidthemakingofzincsoap.Thisresearchaspurposeforsynthesiszincsoapfrompalmoilandzincchloride.Thissurveyresearchlaboratorydidwithseveralstepsas(1)synthesisofsodiumsoapbysaponificatereactionofpalmoilwithsodiumhydroxide(2)synthesisofzincsoapbytrans-saponificationreactionofsodiumsoapwithzincchloride(3)purificationofcompoundsynthesisproductbywashersusewater(4)characterizationofcompoundsynthesisproductincludeactofdeterminingmeltedpointsolubilityexperimentdegradationofzincsoapanalysisqualitativeionzinkdanionchlorideanalysisquantitativezincmetalandsodiummetalwithAAS(5)identificationfunctionclustercompoundsynthesisproductwithspectrophotometricinfrared.Thisproductresearchindicatethatzincsoapcansyntheticfrompalmoilwithzincchloridebytrans-saponificationreaction.Zincsoapsynthesisproductappearancewhitepowderwithmeltedpoint83-91oCsolubilityinbenzene(0020g/mL)chloroform(0003g/mL)varnish(0010g/mL)andunsolubleincoldwaterhotwaterethanolabsoluteacetonen-hexanepetroleum-etheroctanol.AnalysisqualitativezincsoapsynthesisproductcontainsionzincanduncontainsionchlorideanalysisquantitativewithAASindicateamountzinc2056ppmandamountsodium1576ppmasidentificationwithmethodspectrophotometricinfraredcontainstapespecialanioncarboxylic.