ISOLATION AND IDENTIFICATION FLAVONOID COMPOUND FROM THE STEM BARK OF Saccopetalum horsfieldii BENN

Main Author: Mahmiah, Mahmiah; Laboratory of Chemistry, Hang Tuah University, Jl. Arif Rahman Hakim 150 Surabaya
Format: Article info application/pdf eJournal
Bahasa: eng
Terbitan: Universitas Gadjah Mada , 2010
Online Access: http://pdm-mipa.ugm.ac.id/ojs/index.php/ijc/article/view/324
http://pdm-mipa.ugm.ac.id/ojs/index.php/ijc/article/view/324/341
Daftar Isi:
  • Isolation and identification flavonoid compound from the stem bark of Indonesian plant Saccopetalum horsfieldii Benn. Annonaceae family have been done. Extraction was carried out by maseration method using methanol at room temperature, the product was then extracted by n-hexane and etil acetate. Etil acetate extract separation carried out by liquid vacuum column chromatography and flash column chromatography. The product purificated by recristalization using acetone p.a. into yellow solid that having melting point of 224-226 °C. The structure of flavonoid compound was determinated by spectroscopy method : UV-vis, IR, 1H-NMR and 12C-NMR. The flavonoid compound known as quercetin-3,7-dimetil eter or 3,7-dimetoksi quercetin. Keywords: Saccopetalum horsfieldii Benn, flavonoid, chromatography, quercetin